Table 1 Data collection and refinement statistics^a

Data collection

Cell dimensions

Space group

C222

a, b, c (Å)

91.67, 580.82, 177.99

α, β, γ (°)

90, 90, 90

Resolution (Å)

97-6.60 (6.8-6.60)

I/σ(I)

16.62 (1.09)

R_pim^b (%)

4.4 (88.3)

Number of reflections

9402 (766)

Completeness (%)

99.9 (99.9)

Data refinement

Number of atoms (in one monomer)

Protein

3399

Resolution (Å)

97-6.60

Rigid body (with NCS)

Angles (^o)

0.925

Bonds (Å)

0.006

R_work/R_free

0.2863/0.3170

Simulated annealing (with NCS)

t (°K)

1,000

Angles (°)

1.197

Bonds (Å)

0.007

R_work/R_free

0.2731/0.3451